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Partition vs Adsorption

Definition

Partition chromatography separates by differential solubility between two liquid phases (GLC, reversed-phase HPLC). Adsorption chromatography separates by surface binding to a solid (classical TLC on silica).

Related terms

ECD
Electron capture detector. A Ni-63 radioactive source produces a baseline electron current that is reduced when electron-affinic species (halogens, nitro groups, peroxides)...
FID
Flame ionisation detector. A hydrogen-air flame ionises C-H bond containing analytes and a collector electrode reads the ion current. Near-universal for organic...
Isocratic vs Gradient Elution
Isocratic means the mobile-phase composition stays constant through the run; simple, reproducible, but limited resolving power for wide-polarity mixtures. Gradient means the...
Mobile Phase
The solvent or mixture that flows over the stationary phase and carries analytes along. Polarity, viscosity and volatility set the separation; switching...
MSD
Mass Selective Detector. GC-MS or LC-MS detector that identifies analytes by mass spectrum. The confirmation standard for drug and toxicology casework.
Plate Theory
Model that treats a column as a series of theoretical plates. The Height Equivalent to a Theoretical Plate (HETP) measures column efficiency;...
Rf Value
The retention factor, defined as the distance the spot travels divided by the distance the solvent front travels on the same plate....
Stationary Phase
The immobile material the mixture flows past. In paper it is water inside cellulose fibres; in classical column work and TLC it...

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